Preparation and Study the Structure of Pure and Impure Barium Titanate with Zr4+ Ion
Engineering and Technology Journal,
2019, Volume 37, Issue 1B, Pages 21-24
AbstractIn this research, pure and impure barium titanate with Zr4+ ion with two molar ratios x= (5, 10) % have been synthesized by solid-state reaction technique. The powders calculations at two temperatures (950°C and 1400°C). An XRD technique was used in order to study the crystal structure of pure and impure barium titanate, which confirmed the formation of the tetragonal phase of BaTiO3, then calculate the lattice parameters of pure and impure barium titanate, the addition of zirconium ion Zr4+ lead to increases lattice parameters.
 Y. Dang-Hyok, “Tetragonality of barium titanate
powder for a ceramic capacitor application,” Journal of
Ceramic Processing Research, Vol.7, No. 4, p. 343-
 H. Lin, “Structure and Dielectric Properties of
Perovskite- Barium Titanate (BaTiO3),” Ph.D. Theses,
San Jose State University, 2002.
 S.M. Ali and M.M. Najim, “Synthesis and Study
the Dielectric Properties of La-Doped and Undoped
Barium Titanate Nanopowders,” Journal of Eng. &
Tech., Vol. 33, No. 2, 2015.
 S. Pradhan and G.S Roy, “Study the Crystal
Structure and Phase Transition of BaTiO3 – A
Pervoskite,” J. Researcher Vol. 5, No. 3, p.63-67,
 M.M. Najim, “Synthesis and study the structural
and physical properties of Nano-BaTiO3,” Ph.D.
Thesis, University of Technology, School of Applied
 R. Blinc, “Order and Disorder in Perovskites and
Relaxor Ferroelectrics,” Struct. Bond, Vol.124, p. 51-
 J.P.H. Laraa, M.P.Labraa, F.R.B.Hernándeza,
J.A.R. Serranob, E.O.Á. Dávilac, P. Thangarasud,
A.H. Ramirezb, “Structural Evolution and Electrical
Properties of BaTiO3 Doped with Gd3+,” Materials
 M.C. de Andrade, G.N. Carneiro, L.M. Elizabeth,
C. A.Jorge, “Synthesis and Characterization of Barium
Titanate by Solid-State Reaction,” Materials Science
Forum, Vol. 802, p. 285-290, 2014.
 N.M. Zali, C.S. Mahmood, S.M. Mohamad, C.T.
Foo, and J. A.Murshidi, “X-ray Diffraction Study of
Crystalline Barium Titanate Ceramics,” AIP
Conference Proceedings, Vol.1584, No.160, 2014.
 K.E. Oksuz, S. Sen and U. Sen, “Influence of
ZrO2 Addition on the Structure and Dielectric
Properties of BaTiO3 Ceramics,” Special Issue of the
6th International Congress & Exhibition,
 A.E.H. Elbasset, T. Lamcharfi, F. Abdi,
S. Sayouri, L. Mrharrab and Z. Mohamed,
“Characterization of zirconium doping barium titanate
powders by Ramman spectroscopy,” International
Journal of Current Research, Vol. 8, p.25281-25284,
 S. Mahajan, O.P Thakuri, C. Prakash, K.
Sreenivas, “Effect of Zr on dielectric, ferroelectric and
impedance properties of BaTiO3 ceramic,” Bull.
Mater. Sci., Vol. 34, No. 7, p.1483–1489, 2011.
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